Malvern Panalytical Empyrean-XRD

X-ray diffractometers are designed for obtaining the ultimate quality diffraction data, combined with ease of use and flexibility to quickly switch to different applications.
Malvern Panalytical’s X-ray diffractometers are used in many environments, from universities and research institutes to industrial process control labs. Whatever your X-ray diffraction (XRD) need, we offer the right diffractometer, backed up by our worldwide sales and service organization.All our multipurpose diffractometers are all equipped with PreFIX (pre-aligned, fast interchangeable X-ray) modules, making a change in the optical path effortless for the user. For this reason, we offer the most applications on a single diffractometer platform. Read more in our knowledge center about the many exciting XRD applications you can do with our benchtop and floorstanding X-ray diffractometers.

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Description

Empyrean is the only platform that does it all, delivering the best data quality on every sample types. It covers the largest set of X-ray diffraction, scattering and imaging applications in one single instrument. Moreover, Empyrean not only meets the high expectations of scientists and XRD experts today, but will continue to do so as research themes evolve Empyrean is ideal for teaching purposes, thanks to the large doors that open completely, allowing access to the system to several people; but at the same time is perfect to perform measurements in demanding R&D environments in several industries.

Academia 

Get the best data for your publications with Empyrean; train and inspire your students. Acquisition of comprehensive information about a material is the key for successful research. Empyrean will give you the highest data quality, letting you see the finest details of your precious samples by performing non-destructive, cutting-edge characterization studies.

Energy storage/  batteries

Get a better understanding of your battery materials. Analysis of battery material using X-ray diffraction provides component phase purity and the crystallite size of anode and cathode compounds. Empyrean equipped with the GaliPIX3D detector also allows in situ and in operando measurements of long-lasting cells using hard X-radiation.

Pharmaceuticals 

Accomplish advanced characterization of your pharmaceuticals. X-ray powder diffraction, a rapid non-destructive analytical technique, is widely applied in drug discovery, formulation, stability testing and final product quality control. The proven and comprehensive method is available with 21 CFR Part 11 Audit Trail support. Empyrean can also perform in situ non- ambient analysis without manual intervention and high-throughput measurements on well-plates.

Specialty chemicals

Assess crystal structure or structure-property relationship in crystalline and semi-crystalline compounds. Specialty chemicals, also referred to as effect or performance chemicals, are often custom-manufactured materials with unique properties or performance effects to materials or formulation. Empyrean can be used for a detailed phase identification and understanding of these valuable compounds.

Forensics

Reveal the smallest traces of evidence. The use of non-destructive analytical instrumentation plays a key role in today’s forensic laboratories where full chain of custody and data control is desired across all stages of the process. Empyrean can provide information that is vital in criminal investigations and forensic science.

Metals

Determine retained austenite, stress and texture during metal production. Process control and quality control in the metal industry – whether it concerns primary metals or special products – need rapid and accurate chemical analysis as well as microstructural characterization of metals and alloys. Empyrean can take care of these needs.

Nanomaterials

Reveal dimensions and structures in all types of nanomaterials. X-ray scattering and diffraction are powerful and versatile nanometrology tools for the determination of nanoscale dimensions, shapes and structures, as well as the analysis of crystalline phases and local atomic structures. Empyrean delivers most accurate scattering data.

Thin film metrology

Get access to critical parameters of thin films ranging from ultra-thin single layers to complex multilayer stacks. X-ray diffraction and X-ray reflectivity can provide non-destructive, reliable and accurate data for the characterization of thin films. Empyrean enables the determination of ultra-fast reciprocal space maps, X-ray reflectivity and rocking curve analysis.

Malvern-Panalytical X-Ray Machine

Highest data quality on every sample

Praised by scientists for its performance, Empyrean allows them to prepare for synchrotron beam time in the best possible way. The unrivalled collection of sample stages and optical components for Empyrean allows applications to be done in various ways: from ‘simple’ by just adding a few slits and analysis software to a standard geometry, to top performance using dedicated optics, sources and detectors. This is ideal for a multipurpose laboratory: if the need for a certain application increases, data quality and throughput time can be improved by adding dedicated modules.

Highest data quality on every sample

Multipurpose and future proof

“The only thing constant in life is change”. This holds especially in a research environment, where the analytical needs often change with a redirection of the research program. New applications are easily added to an Empyrean system, making it the perfect answer for anything the feature will hold. New and exciting applications are constantly developed on this platform, keeping our customers on the cutting edge of technology.

Multipurpose and future proof

Hybrid PIXel technologies

Malvern Panalytical has always been at the forefront of hybrid detector technology. We were the first company to introduce combined 0D and 1D functionality in silicon strip detectors and to expand the onboard flexibility to 0D-1D-2D-3D. The small pixel size, zero background and the high dynamic range of our hybrid detectors (PIXcel3D and GaliPIX3D) bring with them a revolution in the way XRD applications are treated. No longer is it necessary to maximize intensity or 2D detector size. With a choice of optics and operational radii, you can optimize the configuration to really suit your purpose.

Hybrid PIXel technologies

MultiCore Optics

The newly developed MultiCore Optics featuring the iCore and dCore, greatly simplify the usage of a multipurpose system, bringing automation to a level never been seen before. When switching between measurements the iCore and dCore take care of the work and do not need any human intervention.

MultiCore Optics

PreFIX

PreFIX is our proven proprietary concept that stands for pre-aligned fast interchangeable X-ray modules.

Thanks to this PreFIX concept your diffraction system becomes flexible, fast and future proof. The PreFIX mounting method of optics and stages enables the diffractometer to be reconfigured thanks to a reproducible positioning in three dimensions with microns precision. This allows users to switch between different applications in a matter of minutes, making the Empyrean a real multipurpose diffractometer.

PreFIX

Good laboratory practice

Empyrean with its alignment-free PreFIX modules and measurement and analysis automation possibilities supports anyone who has good laboratory practice (GLP) in mind. In addition, every aspect of the Empyrean package, from the hardware to dedicated analysis solutions, comes with extensive tutorials for novice users yet offers access to all functions for experts.

Good laboratory practice

Customized solutions for X-ray diffraction

The Empyrean is a true multi-purpose instrument, designed to support a wide range of applications. Yet, in the market place we often meet scientists and analysts working with our equipment who would like to extend the possibilities even further, according to their own ideas for their own research. At Malvern Panalytical, we like to support our users in their materials research. We bring them the right solution for complex analytical problems or cost-effective production processes. If you have concepts for new sample holders and stages, optical modules or analytical techniques, discuss your requirements with your local Malvern Panalytical sales representative or submit your request if you need a dedicated solution for your diffraction research. Together we can work on advanced solutions for new requirements, keeping pace with the latest developments in the world of science and research.

Customized solutions for X-ray diffraction

Enclosure Goniometer X-ray source/ Detectors/Stages
Dimensions: 1400 (w) x 1162 (d) x 1947 (h) mm Vertical goniometer, available in theta-theta or alpha-1 geometry Fully ceramic X-ray tubes manufactured by Malvern Panalytical’s specialized factory under cleanroom conditions
Weight: 1150 kg 240 mm radius, interfaces are available to reduce or extend the diffracted beam radius for specific applications Tool free swap of line to point focus
Large doors, allowing access for up to four people simultaneously Maximum usable range (depending on accessories) -111°< 2θ <168° 4 kW generator supporting all current and future X-ray tubes
Meets all relevant worldwide regulations for electrical, mechanical and X-ray safety, with all anode types New generation direct optical encoding system (DOPS 2) for lifetime goniometer accuracy, using precisely aligned Heidenhain encoders and path tracking technology All Empyrean instruments are designed for 60 kV operation, allowing optimal performance for Mo and Ag sources
System is on wheels for easy installation and relocation 2θ linearity equal or better than ±0.01° Hybrid pixel detectors with smallest pixel size available on the market
Automatic recognition of optical modules Angular resolution: 0.026° FWHM on LaB6 Large range of ambient and non-ambient stages
Smallest increment: 0.0001° Angular reproducibility:< 0.0002°

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